最近在看李亚栋院士的那个非
铂催化剂的文章，Zif-8掺杂铁
甲醇120水热4小时。感觉比较危险，各位哪位做过提提经验
https://onlinelibrary.wiley.com/doi/full/10.1002/anie.201702473
Synthesis of Fe(acac)3-0.1@ZIF-8.
Typically, 2-methylimidazole (1314 mg, 16 mmol) was dissolved in 15 ml methanol with stirring in flask A. Zn(NO3)2·6H2O (1190
mg, 4 mmol) and Fe(acac)3 (141 mg, 2.4 mmol) were dissolved in 30 ml methanol under ultrasound for 15 min to form a clear solution
in flask B. Then, flask B was subsequently added into flask A with vigorous stirring for 1h at room temperature. The solution was
transferred into a 100 ml Teflon-lined stainless-steel autoclave and heated at 120 °C for 4h. The obtained product was separated by
centrifugation and washed subsequently with DMF for third and methanol for twice and finally dried at 70 °C under vacuum for
overnight.
